Crystalstructure of N-(2-Cyano-1-Phenylprop-2-en-1-yl)-4-Methylbenzenesulfonamide

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dc.contributor.authorRubinger, M. M. M.
dc.contributor.authorSouza, R. A. C.
dc.contributor.authorGuilardi, S.
dc.contributor.authorTerra, L. R.
dc.contributor.authorTavares, E. C.
dc.contributor.authorEllena, J. A.
dc.date.accessioned2019-03-01T14:00:56Z
dc.date.available2019-03-01T14:00:56Z
dc.date.issued2018-09
dc.description.abstractNew allylsulfonamide is prepared in a four-step synthetic route: the Morita-Baylis-Hillman adduct prepared from benzaldehyde and acrylonitrile is acetylated using acetic anhydride and DMAP. The acetylated product reacts with DABCO displaced by the addition of 4-methylbenzenesulfonamide. The final product is characterized by high-resolution mass spectrometry, infrared, and NMR spectroscopic techniques. The X-ray crystallographic method is used to determine the crystal structure and features of the molecular structure of the compound.en
dc.formatpdfpt-BR
dc.identifier.issn1573-8779
dc.identifier.urihttps://doi.org/10.1134/S0022476618050244
dc.identifier.urihttp://www.locus.ufv.br/handle/123456789/23785
dc.language.isoengpt-BR
dc.publisherJournal of Structural Chemistrypt-BR
dc.relation.ispartofseriesVolume 59, Issue 5, Pages 1192–1194, September 2018pt-BR
dc.rightsPleiades Publishing, Ltd.pt-BR
dc.subjectSynthesispt-BR
dc.subjectX-ray crystallographic analysispt-BR
dc.subjectAllylsulfonamidept-BR
dc.subjectMorita-Baylis-Hillman adductpt-BR
dc.titleCrystalstructure of N-(2-Cyano-1-Phenylprop-2-en-1-yl)-4-Methylbenzenesulfonamideen
dc.typeArtigopt-BR

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